Reaction equation
[C:1]([O-:4])(=[O:3])[CH3:2].[Pb+2:5].O.[C:7]([O-:10])(=[O:9])[CH3:8]>CCCCOCCO>[C:1]([O-:4])(=[O:3])[CH3:2].[Pb+2:5].[C:7]([O-:10])(=[O:9])[CH3:8]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
The hydrate lead acetate is dissolved in butoxyethanol (BuEtOH) (1) at 60° C. The resulting solution is kept at this temperature for two hours, and is cooled down slowly (2) to thereby form a precipitate of dehydrated lead acetate. The precipitation yield can be promoted by further cooling down the vessel containing said solution in an ice bath.
Sources & evidence
- ORD record
- ord-d2912ed95edd4b108b23c3a7feb1bdf4
- Source dataset
- uspto-grants-2001_10
- Patent number
- US06300144B1
Linked notes
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