2-Nitrobenzyl alcohol → (2-Nitrophenyl)methyl N-cyclohexylcarbamate

HRID 383200

Reaction equation

HRID 383200 reaction equation
[N+:1]([C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH2:6][OH:7])([O-:3])=[O:2].[CH:12]1([N:18]=[C:19]=[O:20])[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1.[N+](C1C=CC=CC=1COC(CCCCCCCCN)=O)([O-])=O>C1(C)C=CC=CC=1>[N+:1]([C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH2:6][O:7][C:19]([NH:18][CH:12]1[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1)=[O:20])([O-:3])=[O:2]

Participants

5

Reactant 3

HCID 119232-Nitrobenzyl alcoholHCID 18502Cyclohexyl isocyanateHCID 68713736HCID 68713736, compound

Product 1

HCID 21910133(2-Nitrophenyl)methyl N-cyclohexylcarbamate

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

[[(2-nitrobenzyl)oxy]carbonyl]cyclohexylamine was prepared using 2-nitrobenzylalcohol, cyclohexylisocyanate, and toluene solvent in the same preparation method of [[(2-nitrobenzyl)oxy]carbonyl]octylamine as in Example 1.

Sources & evidence

ORD record
ord-8e00a64c1cbc4761bc809b3331a76e41
Source dataset
uspto-grants-2013_02
Patent number
US08367190B2

Linked notes

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