2,5-Dichloroaniline → 4-amino-N-(2,5-dichlorophenyl)-1,2,5-oxadiazole-3-carboxamide

HRID 386826

Reaction equation

HRID 386826 reaction equation
[NH2:1][C:2]1[C:3]([C:7]([OH:9])=O)=[N:4][O:5][N:6]=1.[Cl:10][C:11]1[CH:17]=[CH:16][C:15]([Cl:18])=[CH:14][C:12]=1[NH2:13]>>[NH2:1][C:2]1[C:3]([C:7]([NH:13][C:12]2[CH:14]=[C:15]([Cl:18])[CH:16]=[CH:17][C:11]=2[Cl:10])=[O:9])=[N:4][O:5][N:6]=1

Participants

3

Reactant 2

HCID 72622,5-DichloroanilineHCID 5474544-Amino-1,2,5-oxadiazole-3-carboxylic acid

Product 1

HCID 585582864-amino-N-(2,5-dichlorophenyl)-1,2,5-oxadiazole-3-carboxamide

Procedure

This compound was prepared according to the procedure of Example 45, Step 1, using 4-amino-1,2,5-oxadiazole-3-carboxylic acid and 2,5-dichloroaniline as the starting materials. LCMS for C9H7Cl2N4O2 (M+H)+: m/z=273.0.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-4957330dc4024c26986f6e9cb76fb5c4
Source dataset
uspto-grants-2013_02
Patent number
US08372870B2

Linked notes

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