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Dimethylamine → 1,3-Dimethyl-8-(2-methoxy-4-dimethylaminosulfonyl-phenyl)-1H,3H-purin-2,6-dione

HRID 3880
Notes
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Reaction equation

HRID 3880 reaction equation
[CH3:1][N:2]1[C:10](=[O:11])[C:9]2[NH:8][C:7]([C:12]3[CH:17]=[CH:16][C:15]([S:18](Cl)(=[O:20])=[O:19])=[CH:14][C:13]=3[O:22][CH3:23])=[N:6][C:5]=2[N:4]([CH3:24])[C:3]1=[O:25].[CH3:26][NH:27][CH3:28]>>[CH3:1][N:2]1[C:10](=[O:11])[C:9]2[NH:8][C:7]([C:12]3[CH:17]=[CH:16][C:15]([S:18]([N:27]([CH3:28])[CH3:26])(=[O:20])=[O:19])=[CH:14][C:13]=3[O:22][CH3:23])=[N:6][C:5]=2[N:4]([CH3:24])[C:3]1=[O:25]
ParticipantsProcedureSources & evidenceReaction notes

Participants

3

Reactant 2

HCID 674DimethylamineHCID 201533401,3-dimethyl-8-(2-methoxy-4-chlorosulfonyl-phenyl)-1H,3H-purin-2,6-dione

Product 1

HCID 201532551,3-Dimethyl-8-(2-methoxy-4-dimethylaminosulfonyl-phenyl)-1H,3H-purin-2,6-dione

Procedure

Prepared analogously to Example 11 from 1,3-dimethyl-8-(2-methoxy-4-chlorosulfonyl-phenyl)-1H,3H-purin-2,6-dione and dimethylamine.

Sources & evidence

ORD record
ord-75a79419a651472b8e61ac37752ac50b
Source dataset
uspto-grants-1988_02
DOI
10.6084/m9.figshare.5104873.v1
On this pageParticipantsProcedureSources & evidenceReaction notes
Patent number
US04722929

Reaction notes

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