HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-ethynylphenyl)acetamide → HCID 24952781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-ethynylphenyl)acetamide | HCID 2726447 | — |
| Reactant | (S)-5-bromo-N-[methyl(oxido)phenyl--sulfanylidene]nicotinamide | HCID 86629466 | — |
| Product | HCID 24952781 | HCID 24952781 | 67.8% |
Reaction Steps
In a manner similar to that described in Example 449, N-(3-ethynyl-phenyl)-acetamide (0.0469 g, 0.443 mmol) and (S)-5-bromo-N-[methyl(oxo)phenyl-λ6-sulfanylidene]nicotinamide (100 mg, 0.295 mmol) were reacted to give the title compound as a solid (83 mg, 0.20 mmol, 67%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383825B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-cf677d504d254127bdfaa6ad39fe3fe5 |
| Source note | uspto-grants-2013_02 |