Ammonia → HCID 178508681, compound

Reaction equation

[NH3:1].[NH2:2][C:3]1[CH:4]=[C:5]([C:11]#[N:12])[C:6](=[CH:9][CH:10]=1)[C:7]#[N:8].C[O-].[Na+]>>[NH2:2][C:3]1[CH:4]=[C:5]2[C:6](=[CH:9][CH:10]=1)[C:7](=[NH:8])[NH:12][C:11]2=[NH:1]

Participants

Reactant 3

HCID 222Ammonia

HCID 925291,2-Benzenedicarbonitrile, 4-amino-

HCID 10942334Sodium Methoxide

Product 1

HCID 178508681HCID 178508681, compound

Procedure

5-Amino-1,3-diiminoisoindoline was synthesized by passing gaseous ammonia through methanolic solution of 4-aminophthalonitrile in the presence of sodium methoxide.

Sources & evidence

ORD record: ord-16eb24294f3c484c86a7974dc38c252d
Source dataset: uspto-grants-2013_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08524891B2

Reaction notes

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