Benzyl Alcohol → Diphenylacetyl-carbamic acid benzyl ester

Reaction equation

[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:19]([OH:26])[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[CH2:19]([O:26][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1

Participants

Reactant 2

HCID 244Benzyl Alcohol

HCID 11264874Diphenylacetyl isocyanate

Product 1

HCID 11131752Diphenylacetyl-carbamic acid benzyl ester

Procedure

The title compound, white solid, m.p. 100-101° C. and MS: m/e=345 (M+) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and benzyl alcohol.

Sources & evidence

ORD record: ord-76a62c26e1d84179a971c89c560434ab
Source dataset: uspto-grants-2004_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06803381B1

Reaction notes

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