1,4-Dibromobutane → Methyl 1-(4-bromobutyl)cyclobutane-1-carboxylate

Reaction equation

[Br:1][CH2:2][CH2:3][CH2:4][CH2:5]Br.[CH3:7][O:8][C:9]([CH:11]1[CH2:14][CH2:13][CH2:12]1)=[O:10]>>[CH3:7][O:8][C:9]([C:11]1([CH2:5][CH2:4][CH2:3][CH2:2][Br:1])[CH2:14][CH2:13][CH2:12]1)=[O:10]

Participants

Reactant 2

HCID 80561,4-Dibromobutane

HCID 136594Cyclobutanecarboxylic acid methyl ester

Product 1

HCID 20334289Methyl 1-(4-bromobutyl)cyclobutane-1-carboxylate

Procedure

1-(4-Bromobutyl)cyclobutane carboxylic acid methyl ester was prepared from 1,4-dibromobutane and cyclobutane carboxylic acid methyl ester using the general procedure described in example 168.

Sources & evidence

ORD record: ord-eb479964ce8f49ac88937d17844dd540
Source dataset: uspto-grants-2004_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06806365B2

Reaction notes

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