Methyl 4-[(acetylsulfanyl)methyl]oxane-4-carboxylate → 1-Acetylsulfanylmethylcyclohexanecarboxylic acid methyl ester

HRID 393736

Reaction equation

HRID 393736 reaction equation
[CH3:1][O:2][C:3]([C:5]1([CH2:11][S:12][C:13](=[O:15])[CH3:14])[CH2:10][CH2:9]O[CH2:7][CH2:6]1)=[O:4].[CH3:16]OC(C1(CI)CCCCC1)=O>>[CH3:1][O:2][C:3]([C:5]1([CH2:11][S:12][C:13](=[O:15])[CH3:14])[CH2:10][CH2:9][CH2:16][CH2:7][CH2:6]1)=[O:4]

Participants

3

Reactant 2

HCID 23448262Methyl 4-[(acetylsulfanyl)methyl]oxane-4-carboxylateHCID 58947958Methyl 1-(iodomethyl)cyclohexanecarboxylate

Product 1

HCID 589479501-Acetylsulfanylmethylcyclohexanecarboxylic acid methyl esterYield 92%

Procedure

Prepared according to the method for the preparation of 4-acetylsulfanylmethyltetrahydropyran-4-carboxylic acid methyl ester, from 1-iodomethylcyclohexanecarboxylic acid methyl ester (20 g), to yield the title compound as a brown gum (15 g, 92%).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-f1fc7002919e45578ab70aacfdbdf934
Source dataset
uspto-grants-2004_10
Patent number
US06809100B2

Linked notes

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