Cetyl Alcohol → Phenyl butyrate

HRID 393766

Reaction equation

[CH2:1]([OH:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]CCCCCCCCCC.C1([CH2:24][CH2:25][CH2:26][C:27]([O-])=[O:28])C=CC=CC=1>>[C:1]1([O:17][C:27](=[O:28])[CH2:26][CH2:25][CH3:24])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

Reactant 2

HCID 2682Cetyl Alcohol

HCID 220532644-Phenylbutyrate

Product 1

HCID 20354Phenyl butyrate

Conditions

Temperature: 70 °C

Procedure

65 g of white petrolatum (Riedel-de Haen), 15 g of cetyl alcohol (Riedel-de Haen), 260 g of soft paraffin (Merck), 155 g of liquid paraffin (Merck), and 5 g of 4-phenylbutyrate (Merck) were mixed in a beaker and heated at 70° C. to form a paste. The paste was stirred at 400 rpm for 1 hour, and then cooled at room temperature.

Workup

customto form a paste
temperaturecooled at room temperature

Sources & evidence

ORD record: ord-e72f6910a1a14f149601665766f45e87
Source dataset: uspto-grants-2004_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06809118B2

Linked notes

Loading…