4-Methoxy-3-nitrobenzoic acid → n1-(3-Nitro-4-methoxybenzoyl)-n2-(4-tert-butylbenzoyl)-1,2-benzenediamine

HRID 395775

Reaction equation

HRID 395775 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[O:13][CH3:14])[C:7]([OH:9])=O)([O-:3])=[O:2].[C:15]([C:19]1[CH:34]=[CH:33][C:22]([C:23]([NH:25][C:26]2[C:27]([NH2:32])=[CH:28][CH:29]=[CH:30][CH:31]=2)=[O:24])=[CH:21][CH:20]=1)([CH3:18])([CH3:17])[CH3:16]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[O:13][CH3:14])[C:7]([NH:32][C:27]1[C:26]([NH:25][C:23](=[O:24])[C:22]2[CH:33]=[CH:34][C:19]([C:15]([CH3:17])([CH3:16])[CH3:18])=[CH:20][CH:21]=2)=[CH:31][CH:30]=[CH:29][CH:28]=1)=[O:9])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 666404-Methoxy-3-nitrobenzoic acidHCID 1133079N-(2-aminophenyl)-4-tert-butylbenzamide

Product 1

HCID 31973964n1-(3-Nitro-4-methoxybenzoyl)-n2-(4-tert-butylbenzoyl)-1,2-benzenediamineYield 84%

Procedure

Using the procedure described in Example 102, Part A, 3-nitro-4-methoxybenzoic acid (2.8 mmol) and N1-(4-tert-butylbenzoyl)-1,2-benzenediamine (1.9 mmol) yielded 0.70 mg (84%) of the title compound.

Sources & evidence

ORD record
ord-3a199c182a714adf97d315d18da864b8
Source dataset
uspto-grants-2003_08
Patent number
US06605626B2

Linked notes

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