Thionyl Chloride → Cycloheptylmethanesulfonyl chloride

Reaction equation

[CH:1]1([CH2:8][S:9]([O-:12])(=O)=[O:10])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Na+].S(Cl)([Cl:16])=O>>[CH:1]1([CH2:8][S:9]([Cl:16])(=[O:12])=[O:10])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

Reactant 2

HCID 24386Thionyl Chloride

HCID 23670189Sodium cycloheptylmethanesulfonate

Product 1

HCID 23000687Cycloheptylmethanesulfonyl chloride

Procedure

The subtitle compound was prepared by the method of Preparation 58 from sodium cycloheptylmethanesulfonate [Preparation 67] and thionyl chloride, to afford cycloheptylmethanesulfonyl chloride as a colourless oil.

Sources & evidence

ORD record: ord-d4a46cf96c024383aaa5e799d2e637db
Source dataset: uspto-grants-2003_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06610707B1

Reaction notes

Loading…