Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Chlorobenzamide | HCID 12084 | — |
| Reactant | Sulfur trioxide triethylamine complex | HCID 222301 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 4-Chlorobenzonitrile | HCID 12163 | 92% |
Reaction Steps
A suspension of 50 mmol of 4-chlorobenzamide and 125 mmol of triethylamine-sulphur trioxide in 75 ml of triethylamine was stirred at 89° C. for 6 hours. The working up was effected as described under Example 1a). Yield: 92% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05817827 |
|---|
| Source dataset | uspto-grants-1998_10 |
|---|
| ORD ID | ord-b2757f70e3944870b6dfb8a9c6b718e2 |
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| Source note | uspto-grants-1998_10 |
|---|
