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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 399296Generated: October 27, 2026

1,3-Cyclopentadiene, 5-(1-methylethylidene)- → HCID 131720872, compound

https://huagongshe.com/reaction/399296

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,3-Cyclopentadiene, 5-(1-methylethylidene)-HCID 137467—
ReactantPotassium, (diphenylmethyl)-HCID 11858962—
SolventTetrahydrofuranHCID 8028—
ProductHCID 131720872HCID 131720872—

Reaction Conditions

Temperature25 °C

Reaction Steps

Potassium diphenylmethanide (5.72 g, 27.8 mmols) in about 50 mL of THF was slowly added to 6,6-dimethylfulvene (2.94 g, 27.8 mmols) in about 100 mL of THF at about 25 C. The reaction mixture was stirred at about 25° C. for about 16 hours. The solvent was removed under reduced pressure to give the desired product as a sticky, oily solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05817849
Source datasetuspto-grants-1998_10
ORD IDord-977dbb3c7fbe44209e362dc473b9d505
Source noteuspto-grants-1998_10