4-Hydroxy-4'-nitrobiphenyl → N,N-bis-(isopropyl)-2[[4'-nitro-(1,1'-biphenyl)-4-yl]oxy]-acetamide

Participants

Role	Name	HCID	Charge
Reactant	4-Hydroxy-4'-nitrobiphenyl	HCID 138078	—
Reactant	2-Bromo-N,N-diisopropylacetamide	HCID 10900191	—
Product	N,N-bis-(isopropyl)-2[[4'-nitro-(1,1'-biphenyl)-4-yl]oxy]-acetamide	HCID 21841479	84.5%

Reaction Steps

The product was prepared as in Example 2, Stage A starting with 900 mg of 4'-hydroxy-(4-nitro biphenyl) (Aldrich) and 958 mg of N,N-bis-(isopropyl)-2-bromo-acetamide (Preparation 8) to obtain 1.26 g of the expected product.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US05827887
Source dataset	uspto-grants-1998_10
ORD ID	ord-4b1bbf3a66324fc88b583320d996d174
Source note	uspto-grants-1998_10