2,4-Dinitroanisole → 2,4-Diaminoanisole
Reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([N+:9]([O-])=O)=[CH:5][C:4]=1[N+:12]([O-])=O>CC#N>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH2:9])=[CH:5][C:4]=1[NH2:12]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
4-Methoxy-benzene-1,3-diamine (D-3) was synthesized following the general scheme above starting from 1-methoxy-2,4-dinitro-benzene. Yield (quant.). HPLC ret. time 0.31 min, 10-99% CH3CN, 5 min run.
Workup
- customYield (quant.)
Sources & evidence
- ORD record
- ord-783a2e28861548c29777c24399395ae1
- Source dataset
- uspto-grants-2014_06
- Patent number
- US08741925B2
Reaction notes
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