HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperonal → 4-(1,3-benzodioxol-5-ylmethyl)-N-phenylpiperazine-1-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperonal | HCID 8438 | — |
| Reactant | N-phenylpiperazine-1-carboxamide | HCID 7015289 | — |
| Product | 4-(1,3-benzodioxol-5-ylmethyl)-N-phenylpiperazine-1-carboxamide | HCID 675027 | — |
Reaction Steps
The title compound was prepared from piperazine-1-carboxylic acid phenylamide and benzo[1,3]dioxole-5-carbaldehyde. 1H NMR (400 MHz, CDCl3): 7.36-7.24 (m, 4H), 7.05-6.99 (m, 1H), 6.86 (br s, 1H), 6.77-6.72 (m, 2H), 6.43 (br s, 1H), 5.95 (s, 2H), 3.50-3.46 (m, 4H), 3.43 (s, 2H), 2.46-2.42 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08530476B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-d42b645102fb462481a11dbad67c07ec |
| Source note | uspto-grants-2013_09 |