Phosphoric Acid → Zirconium phosphate

HRID 41228

Reaction equation

[P:1]([O-:5])([O-:4])([O-:3])=[O:2].[P:6](=[O:10])([OH:9])([OH:8])[OH:7].[Zr:11]>>[P:1]([O-:5])([O-:4])([O-:3])=[O:2].[Zr+4:11].[P:6]([O-:10])([O-:9])([O-:8])=[O:7].[P:1]([O-:5])([O-:4])([O-:3])=[O:2].[P:1]([O-:5])([O-:4])([O-:3])=[O:2].[Zr+4:11].[Zr+4:11]

Participants

Reactant 3

HCID 1004Phosphoric Acid

HCID 1061Phosphate

HCID 23995Zirconium

Product 1

HCID 160986Zirconium phosphate

Conditions

Temperature: 350 °C

Procedure

A zirconium phosphate film was prepared by adding a stoichometric amount of phosphate in the form of phosphoric acid to a solution of zirconium bound to PEI. The solution was then spin coated onto a glass slide and thermally treated at 1° C. to 120° C. with a dwell time of 30 minutes followed by heating to 350° C. at 1° C./minute with a dwell time of 30 minutes followed by heating to 450° C. at 1° C./minute with a dwell time of 1 hour and then cooling to 25° C.

Workup

additionthermally treated at 1° C. to 120° C. with a dwell time of 30 minutes
temperatureby heating to 450° C. at 1° C./minute with a dwell time of 1 hour
temperaturecooling to 25° C.

Sources & evidence

ORD record: ord-cf4b6531eeb34d11a932e26327e1f566
Source dataset: uspto-grants-2013_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08530554B1

Linked notes

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