Water → Laurolactam

HRID 41343

Reaction equation

HRID 41343 reaction equation
[C:1]1(=[N:13]O)[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[OH2:15]>>[C:1]1(=[O:15])[NH:13][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]1

Participants

3

Reactant 2

HCID 962WaterHCID 136762Cyclododecanone, oxime

Product 1

HCID 13690Laurolactam

Procedure

For example, after the reaction of cyclododecanone oxime, the reaction can be worked up by adding water, extracting a product with an organic solvent and then evaporating the solvent to give laurolactam, which can be further separated and purified by, for example, distillation or crystallization.

Workup

  1. customthe reaction
  2. extractionextracting a product with an organic solvent
  3. customevaporating the solvent

Sources & evidence

ORD record
ord-bf9970b51c7248ce8751f7ff38820cf3
Source dataset
uspto-grants-2013_09
Patent number
US08530645B2

Linked notes

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