HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-n-Octadecyloxybenzoic acid → 4-(trans-3-Decenyloxy)-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-n-Octadecyloxybenzoic acid | HCID 139993 | — |
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | Methyl-4-(trans-3-decenyloxy)-benzoate | HCID 18521096 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(trans-3-Decenyloxy)-benzoic acid | HCID 18521103 | — |
Reaction Steps
Ester 35h (600 mg, 2.07 mmol), and lithium hydroxide monohydrate (867 mg, 20.7 mmol) in 20 ml methanol were reacted according to the procedure for compound 36a. The yield was 500 mg (87%) of a white powder which was not quite pure (95%). The product was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06569504B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-d8c3667c163749e7a921df5f12e71ed3 |
| Source note | uspto-grants-2003_05 |