HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 414293Generated: October 26, 2026
Triphenylphosphine → (2,3,4,5,6-Pentafluorophenyl)methyl-triphenyl-phosphonium;bromide
https://huagongshe.com/reaction/414293
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Pentafluorobenzyl bromide | HCID 74484 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | (2,3,4,5,6-Pentafluorophenyl)methyl-triphenyl-phosphonium;bromide | HCID 21282127 | — |
Reaction Steps
The toluene solution from Stage 1 was mixed with triphenyl phosphine (1 g) and heated at 130° C. for 3 hours. After cooling, the solution was diluted with diethyl ether (5 cm3) and the title compound filtered off, washed with hexane (4×5 cm3) and dried by suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04791139 |
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| Source dataset | uspto-grants-1988_12 |
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| ORD ID | ord-071913ea308748ad9b60322c80e9fd44 |
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| Source note | uspto-grants-1988_12 |
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