2,4,5,6-Tetrachloropyrimidine → N-(2,5,6-Trichloro-pyrimidin-4-yl)-N-methylmethanesulfonamide

HRID 415446

Reaction equation

[CH3:1][NH:2][S:3]([CH3:6])(=[O:5])=[O:4].[Cl:7][C:8]1[N:13]=[C:12]([Cl:14])[C:11]([Cl:15])=[C:10](Cl)[N:9]=1>>[Cl:7][C:8]1[N:9]=[C:10]([N:2]([CH3:1])[S:3]([CH3:6])(=[O:5])=[O:4])[C:11]([Cl:15])=[C:12]([Cl:14])[N:13]=1

Participants

Reactant 2

HCID 156902,4,5,6-Tetrachloropyrimidine

HCID 97632N-Methylmethanesulfonamide

Product 1

HCID 86624849N-(2,5,6-Trichloro-pyrimidin-4-yl)-N-methylmethanesulfonamide

Procedure

Following a procedure similar to that of Method 32, the title compound was prepared from N-methylmethanesulfonamide and 2,4,5,6-tetrachloropyrimidine. MS: 290 (M+1).

Sources & evidence

ORD record: ord-b2223e9210a845b18c70181873d007e2
Source dataset: uspto-grants-2012_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08088784B2

Linked notes

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