Hydrochloric Acid → 1,3,5-Tris-(p-(dec-1-yloxycarbonyl)-anilino)-s-triazine

Participants

Reaction Conditions

Reaction Steps

83 g of decyl p-aminobenzoate and 18.5 g of cyanuric chloride in 1,000 ml of xylene were heated at 140° C. for 8 hours. After the evolution of hydrogen chloride was complete, the reaction solution was cooled to 90° C., washed twice with saturated sodium bicarbonate solution and once with water, and then cooled to room temperature. The white crystals precipitated were filtered off under suction and dried.

Provenance & Evidence