HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylfuran → 1-Methyl-10-oxa-tricyclo[5.2.1.0*2,6*]dec-8-ene-3,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylfuran | HCID 10797 | — |
| Reactant | 2-Cyclopentene-1,4-dione | HCID 70258 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-Methyl-10-oxa-tricyclo[5.2.1.0*2,6*]dec-8-ene-3,5-dione | HCID 58288601 | — |
Reaction Steps
A mixture of 4-cyclopentene-1,3-dione (10 g, 104 mmol) and 2-methylfuran (15 ml) are stirred at room temperature for 3 days. Methanol (50 ml) is then added and the solid is collected and dried on a Buchner funnel to give 1-methyl-10-oxa-tricyclo[5.2.1.0*2,6*]dec-8-ene-3,5-dione (14.3 g)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08530667B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-31f574acb1d14478b81e748c79a80f90 |
| Source note | uspto-grants-2013_09 |