Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Hexafluoropropylene | HCID 8302 | — |
| Product | CCl3CF2CHFCF3 | HCID 12829385 | — |
Reaction Steps
A 0.5 inch (12.7 mm) by 40 inch (101.6 cm) plug flow reactor that is packed with Helipack Monel support is heated to 290° C. A 50/50 (molar %) mixture of hexafluoropropene and chloroform is fed into the reactor at about 1.5 g/min. The reactor pressure is maintained at 100 psig. The effluent from the reactor is fed into a distillation column and the unreacted reagents removed by distillation and recycled. The product CCl3CF2CHFCF3 is used in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08530709B2 |
|---|
| Source dataset | uspto-grants-2013_09 |
|---|
| ORD ID | ord-e25e851eb2fd41f9bfbe6fa77cb92408 |
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| Source note | uspto-grants-2013_09 |
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