HuagongsheHuagongshe Chemistry Print Report · For research reference only
Monoethyl malonate → HCID 178516627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Monoethyl malonate | HCID 70615 | — |
| Reactant | 4-(Thiomorpholin-4-yl)benzaldehyde | HCID 15369093 | — |
| Reactant | Sodium t-butoxide | HCID 23676156 | — |
| Reactant | 1-Isocyano-2-methylpropan-2-yl methyl carbonate | HCID 25267464 | — |
| Reactant | HCID 178507353 | HCID 178507353 | — |
| Product | HCID 178516627 | HCID 178516627 | — |
Reaction Steps
The compound was synthesized starting from 1H-benzo[d]imidazol-5-amine (0.963 g, 7.24 mmol), 4-thiomorpholinobenzaldehyde (1.5 g, 7.24 mmol), 2-(ethoxycarbonyl)acetic acid (0.957 g, 7.24 mmol), 1-isocyano-2-methylpropan-2-yl methyl carbonate (1.13 g, 7.24 mmol) and sodium tert.-butoxide (0.77 g, 6.87 mmol) according to method 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08530670B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-225648086b724bd2b3dbff6a448ccb30 |
| Source note | uspto-grants-2013_09 |