HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl malonate → HCID 178515848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl malonate | HCID 21883978 | — |
| Reactant | Sodium t-butoxide | HCID 23676156 | — |
| Reactant | 1-Isocyano-2-methylpropan-2-yl methyl carbonate | HCID 25267464 | — |
| Reactant | 4-(4-Oxocyclohexyl)benzaldehyde | HCID 86670880 | — |
| Reactant | HCID 178507353 | HCID 178507353 | — |
| Product | HCID 178515848 | HCID 178515848 | — |
Reaction Steps
The compound was synthesized starting from 1H-benzo[d]imidazol-5-amine (0.803 g, 6.04 mmol), 4-(4-oxocyclohexyl)benzaldehyde (1.5 g, 6.04 mmol), mono-tert-butyl malonate (0.97 g, 6.04 mmol), 1-isocyano-2-methylpropan-2-yl methyl carbonate (0.95 g, 6.04 mmol) and sodium tert.-butoxide (0.60 mg, 5.35 mmol) according to method 5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08530670B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-08d7ac3e2aaf4b138490cb7faa4c7e3b |
| Source note | uspto-grants-2013_09 |