HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodocyclopentane → 3-Cyclopentyl-1H-indol-6-ylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodocyclopentane | HCID 73784 | — |
| Reactant | 6-Nitro-1H-indole | HCID 78502 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 3-Cyclopentyl-1H-indol-6-ylamine | HCID 57470201 | — |
Reaction Steps
3-Cyclopentyl-1H-indol-6-ylamine (B-15) was synthesized following the general scheme above starting from 6-nitroindole and iodo-cyclopentane. Overall yield (16%). HPLC ret. time 2.39 min, 10-99% CH3CN, 5 min run; ESI-MS 201.5 m/z (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101767B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-4a826e1b177a47d4972292c7c179bb13 |
| Source note | uspto-grants-2012_01 |