HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → N-(4,5-dichloro-2-nitrophenyl)ethane-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 2,4,5-Trichloronitrobenzene | HCID 6983 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-(4,5-dichloro-2-nitrophenyl)ethane-1,2-diamine | HCID 54360568 | — |
Reaction Steps
0.13 mole (30.6 g) of 2,4,5-trichloronitrobenzene is added to a solution of 78 g of ethylenediamine in 100 ml of 96° ethanol and 117 ml of water. After heating under reflux for 1 h 30 min, the reaction mixture is cooled. After dilution with iced water, the expected product precipitates. It melts as 84° C.-87° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04725283 |
| Source dataset | uspto-grants-1988_02 |
| ORD ID | ord-b8234a4b6b1c4b76ac1f1dde36971aea |
| Source note | uspto-grants-1988_02 |