Methanol → HCID 58484330, compound

HRID 42692

Reaction equation

HRID 42692 reaction equation
Cl[C:2]1[N:7]([CH3:8])[C:6](=[O:9])[N:5]([CH3:10])[C:4](=[O:11])[C:3]=1[CH:12]=[O:13].[CH3:14][OH:15]>>[CH3:14][O:15][C:2]1[N:7]([CH3:8])[C:6](=[O:9])[N:5]([CH3:10])[C:4](=[O:11])[C:3]=1[CH:12]=[O:13]

Participants

3

Reactant 2

HCID 887MethanolHCID 3199716-Chloro-5-formyl-1,3-dimethyluracil

Product 1

HCID 58484330HCID 58484330, compound

Procedure

The process described in Method C was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.270 g, 1.33 mmol) and methanol were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of n-hexane:ethyl acetate (4:1) as the eluent.

Sources & evidence

ORD record
ord-c85dff6070af47f89ad63f95a7464379
Source dataset
uspto-grants-2013_09
Patent number
US08536210B2

Linked notes

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