O-Methylhydroxylamine → cyclohexenyl-ethanone O-methyl-oxime

HRID 42725

Reaction equation

HRID 42725 reaction equation
[C:1]1([C:7](=O)[CH3:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1.[CH3:10][O:11][NH2:12]>C(O)(=O)C>[CH3:10][O:11][N:12]=[C:7]([C:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1)[CH3:8]

Participants

4

Conditions

Temperature
24 °C

Procedure

To a stirred solution of a cyclohexenyl-ethanone (0.06 mmol), in acetic acid (500 μl) was added methoxyamine (4.7 mg). The reaction mixture was stirred at 24° C. for 48 h under nitrogen to obtain the cyclohexenyl-ethanone O-methyl-oxime.

Sources & evidence

ORD record
ord-57036d9ef90e40e0a656d26d4659e650
Source dataset
uspto-grants-2013_09
Patent number
US08536215B2

Linked notes

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