O-Methylhydroxylamine → cyclohexenyl-ethanone O-methyl-oxime
Reaction equation
[C:1]1([C:7](=O)[CH3:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1.[CH3:10][O:11][NH2:12]>C(O)(=O)C>[CH3:10][O:11][N:12]=[C:7]([C:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1)[CH3:8]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 24 °C
Procedure
To a stirred solution of a cyclohexenyl-ethanone (0.06 mmol), in acetic acid (500 μl) was added methoxyamine (4.7 mg). The reaction mixture was stirred at 24° C. for 48 h under nitrogen to obtain the cyclohexenyl-ethanone O-methyl-oxime.
Sources & evidence
- ORD record
- ord-57036d9ef90e40e0a656d26d4659e650
- Source dataset
- uspto-grants-2013_09
- Patent number
- US08536215B2
Reaction notes
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