4-(3-Methoxyphenyl)but-3-en-2-one → HCID 14128157, compound

Reaction equation

[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11](=[O:17])[CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])[CH:6]=[CH:7][CH:8]=1.COC1C=C(C=CC(=O)C)C=CC=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:9][CH2:10][C:11](=[O:17])[CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])[CH:6]=[CH:7][CH:8]=1

Participants

Reactant 2

HCID 1820074-(3-Methoxyphenyl)but-3-en-2-one

HCID 53636343HCID 53636343, compound

Product 1

HCID 14128157HCID 14128157, compound

Procedure

Following the procedure of Example 15 and substituting an equivalent quantity of 1-(3-methoxyphenyl)-1-octen-3-one for 4-(3-methoxyphenyl)-3-buten-2-one there was obtained as the product 1-(3-methoxyphenyl)octan-3-one as a colorless oil.

Sources & evidence

ORD record: ord-7271bcbdc29044d1993bceb145ad2cb2
Source dataset: uspto-grants-1988_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04725602

Reaction notes

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