HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-pyridylacetate → 1-Piperidineacetic acid, ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-pyridylacetate | HCID 75960 | — |
| Reactant | Ethyl 2-(piperidin-3-yl)acetate | HCID 2760464 | — |
| Product | 1-Piperidineacetic acid, ethyl ester | HCID 643466 | — |
Reaction Steps
The reaction was run in the same manner as ethyl 3-piperidinylacetate, starting with commercially available ethyl-2-pyridylacetate (4.00 g; 24.5 mmol). This gave ethyl 2-piperidinylacetate (2.41 g) as a light yellow oil without further purification. MS m/z (positive ion) 172 (MH+; 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664271B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-885d55a01d27437bb29c8817847259b2 |
| Source note | uspto-grants-2003_12 |