HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4-nitrophenyl)pentanamide → N-(4-aminophenyl)pentanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4-nitrophenyl)pentanamide | HCID 3762929 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(4-aminophenyl)pentanamide | HCID 1725711 | — |
Reaction Steps
A solution of 4'-nitrovaleranilide (13.33 g., 0.06 mole) in absolute ethanol (750 ml.) is hydrogenated over 10% palladium on charcoal (2 g.) until the theoretical absorption is achieved. The catalyst is removed and the solvent is removed in vacuo. The residue is recrystallized from butyl chloride to yield 9.0 g., m.p. 81°-83° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04006233 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-8c20ac76b3604360b3c9fcffec14b3fe |
| Source note | uspto-grants-1977_02 |