HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotriethylsilane → 3-Triethylsilyl-2-oxazolidinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotriethylsilane | HCID 13819 | — |
| Reactant | 2-Oxazolidinone | HCID 73949 | — |
| Product | 3-Triethylsilyl-2-oxazolidinone | HCID 21454776 | — |
Reaction Steps
Following the previous example, but replacing the trimethylchlorosilane with triethylchlorosilane (63.3 g; 0.42 mol) and operating under similar conditions, the result is the compound of the above heading; a colourless fluid liquid, obtained with a similar yield. 2-oxazolidinone, calculated: 42.82%; found: 42.70%. Distils at 100° C between 2 and 4 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04007168 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-ede3c3d0c1ca43f09684b307132c2b8e |
| Source note | uspto-grants-1977_02 |