HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride → Dilauryl Ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride | HCID 6356 | — |
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | 1-Dodecanol | HCID 8193 | — |
| Product | Dilauryl Ether | HCID 20667 | — |
| Product | (Z)-3-chloroprop-1-en-1-ol | HCID 15676292 | — |
Reaction Steps
185 g of glycerol epichlorhydrin are reacted with one mole, i.e., 186 g of dodecanol at 75-80° C in the presence of 1.5 ml of an acetic acid complex containing 36% BF3. Dodecyl ether of polyepichlorohydrin having the following formula is obtained:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009255 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-ed296078d4924863935e1c4532039c27 |
| Source note | uspto-grants-1977_02 |