HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → N,N'-Dodecamethylenebis(4-trifluoromethoxybenzamide)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1,12-Dodecanediamine | HCID 17727 | — |
| Reactant | 4-(Trifluoromethoxy)benzoyl Chloride | HCID 142110 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | N,N'-Dodecamethylenebis(4-trifluoromethoxybenzamide) | HCID 21452860 | — |
Reaction Steps
m.p. 158°-159° C., 11.3 g., was prepared as in Example 1 using 24.8 g. of 4-trifluoromethoxybenzoyl chloride in 150 ml. of ethylene dichloride, 10.0 g. of 1,12-dodecanediamine, 60 ml. of 10% aqueous potassium hydroxide solution, 350 ml. of ethylene dichloride and recrystallization twice from ethanol and once from isopropyl alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009208 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-dcc3d143b4c94612acec4c4e25b57104 |
| Source note | uspto-grants-1977_02 |