Calcium epoxysuccinate → Epoxysuccinic acid

HRID 436910

Reaction equation

HRID 436910 reaction equation
[O:1]1[CH:6]([C:7]([O-:9])=[O:8])[CH:2]1[C:3]([O-:5])=[O:4].[Ca+2]>P(OCCCCCCCC)(OCCCCCCCC)(OCCCCCCCC)=O>[O:1]1[CH:6]([C:7]([OH:9])=[O:8])[CH:2]1[C:3]([OH:5])=[O:4]

Participants

3

Reactant 1

HCID 13538056Calcium epoxysuccinate

Product 1

HCID 86022Epoxysuccinic acid

Reagents, catalysts & solvents 1

HCID 15733Trioctyl phosphateSolvent

Procedure

The yield in the reaction effected in trioctyl phosphate amounted to 96%. From 2 moles of acid calcium epoxysuccinate, 507 g. of free epoxysuccinic acid in aqueous solution were obtained.

Workup

  1. customThe yield in the reaction

Sources & evidence

ORD record
ord-f5a6504601f24f0092170cad4a438d02
Source dataset
uspto-grants-1977_06
Patent number
US04028407

Linked notes

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