Calcium epoxysuccinate → Epoxysuccinic acid
Reaction equation
[O:1]1[CH:6]([C:7]([O-:9])=[O:8])[CH:2]1[C:3]([O-:5])=[O:4].[Ca+2]>P(OCCCCCCCC)(OCCCCCCCC)(OCCCCCCCC)=O>[O:1]1[CH:6]([C:7]([OH:9])=[O:8])[CH:2]1[C:3]([OH:5])=[O:4]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
The yield in the reaction effected in trioctyl phosphate amounted to 96%. From 2 moles of acid calcium epoxysuccinate, 507 g. of free epoxysuccinic acid in aqueous solution were obtained.
Workup
- customThe yield in the reaction
Sources & evidence
- ORD record
- ord-f5a6504601f24f0092170cad4a438d02
- Source dataset
- uspto-grants-1977_06
- Patent number
- US04028407
Reaction notes
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