HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → 3-Methyl-2-buten-1-OL
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Isobutane | HCID 6360 | — |
| Reactant | Butane | HCID 7843 | — |
| Reactant | 1-Butene | HCID 7844 | — |
| Reactant | 1,3-Butadiene | HCID 7845 | — |
| Reactant | Isobutylene | HCID 8255 | — |
| Reactant | trans-2-BUTENE | HCID 62695 | — |
| Reactant | cis-2-BUTENE | HCID 5287573 | — |
| Product | 3-Methyl-2-buten-1-OL | HCID 11173 | — |
| Product | 3-Methyl-3-buten-1-ol | HCID 12988 | — |
Reaction Steps
The procedure of Example 1 was repeated except for using 150 ml of spent BB (composition: isobutene 47.3%, isobutane 2.2%, n-butane 8.9%, butene-1 27.6%, trans-2-butene 8.8%, cis-2-butene 4.4% and butadiene 0.87%) as a isobutene source in place of isobutene. Conversion of paraformaldehyde was 97.0 mole%. There were obtained 62.0 mole% of 3-methyl-3-butene-1-ol and 7.1 mole% of 3-methyl-2-butene-1-ol based on the paraformaldehyde reacted.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028424 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-234a96b099dc442d87cf6be6d7a40e74 |
| Source note | uspto-grants-1977_06 |