Sulfuryl chloride → N-(2-chlorobenzyl)-2,2-dioxo-1,2,3-oxathiazolidine

Reaction equation

[OH:1][CH2:2][CH2:3][NH:4][CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[Cl:12].[S:13](Cl)(Cl)(=[O:15])=[O:14]>>[Cl:12][C:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=1[CH2:5][N:4]1[CH2:3][CH2:2][O:1][S:13]1(=[O:15])=[O:14]

Participants

Reactant 2

HCID 24648Sulfuryl chloride

HCID 35615492-(2-Chloro-benzylamino)-ethanol

Product 1

HCID 15227704N-(2-chlorobenzyl)-2,2-dioxo-1,2,3-oxathiazolidine

Procedure

contacting N-hydroxyethyl-2-chlorobenzylamine with sulfuryl chloride and an organic base to give N-(2-chlorobenzyl)-2,2-dioxo-1,2,3-oxathiazolidine, and

Sources & evidence

ORD record: ord-2d449fd4535b44aa898e300beb071e7c
Source dataset: uspto-grants-1996_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05516910

Reaction notes

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