HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → N-(tert-butoxycarbonyl)piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Tert-butyl 1-chloroethyl carbonate | HCID 13557091 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-(tert-butoxycarbonyl)piperidine | HCID 7010304 | — |
Reaction Steps
The procedure is as in Example 7, but with 8.5 g (0.1 mole) of piperidine, 60 ml of THF, 20 ml of saturated aqueous K2CO3 solution and 0.11 mole of α-chloroethyl tert-butyl carbonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04725680 |
| Source dataset | uspto-grants-1988_02 |
| ORD ID | ord-c4542c72534e465fbfebfb91c898577a |
| Source note | uspto-grants-1988_02 |