HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethyl-1,3-Hexanediol → 2-Ethyl-1-triethoxysiloxy-3-hexanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethyl-1,3-Hexanediol | HCID 7211 | — |
| Reactant | Dicyclohexylamine | HCID 7582 | — |
| Reactant | Triethoxychlorosilane | HCID 78398 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Ethyl-1-triethoxysiloxy-3-hexanol | HCID 53757268 | 50% |
Reaction Steps
2-Ethyl-1,3-hexanediol was mixed with chlorotriethoxysilane and dicyclohexylamine in a 1:1:1 ratio at 0° C. in absolute ethanol. The resulting product, 2-ethyl-1-triethoxysiloxy-3-hexanol, was obtained in 50% yield and was dissolved to a 10% by weight solution in a 50/50 by volume mixture of ethanol/cyclomethicone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05891914 |
| Source dataset | uspto-grants-1999_04 |
| ORD ID | ord-91f0fc7233b84088ae42805e4afe647b |
| Source note | uspto-grants-1999_04 |