Phosphorus → Phenyl benzoate
Reaction equation
[C:1]1([C:7](=O)[C:8]([O:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3]C=1.[P]>C(Cl)(Cl)Cl>[C:8]([O:10][C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1)(=[O:9])[C:7]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:1]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
The decarbonylation reaction of phenyl phenylglyoxylate (PPG) was repeated in the manner as described in Example 79, except that the organic phosphorus compound set forth in Table 12 was employed and the amount of chloroform was changed as set forth in Table 12. The results are also set forth in Table 12.
Sources & evidence
- ORD record
- ord-f7fbf6f2a6444ceea29bd3e415ab91da
- Source dataset
- uspto-grants-1999_04
- Patent number
- US05892091
Reaction notes
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