HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isocyanate → N-(3-Cyano-5-methylthiophen-2-ylcarbamoyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isocyanate | HCID 78210 | — |
| Reactant | 2-Amino-5-methyl-3-thiophenecarbonitrile | HCID 689056 | — |
| Product | N-(3-Cyano-5-methylthiophen-2-ylcarbamoyl)benzamide | HCID 57456905 | — |
Reaction Steps
Prepared as in Example 1a from 2-amino-5-methylthiophene-3-carbonitrile and benzoyl isocyanate as a white solid. 1H NMR (400 MHz, DMSO-d6) δ2.36 (d, J=1.2 Hz, 3H), 6.89 (d, J=1.2 Hz, 1H), 7.55 (t, J=8.0 Hz, 2H), 7.66 (d, J=7.2 Hz, 1H), 8.03-8.01 (m, 2H), 11.60 (brs, 1H), 12.08 (bs, 1H). MS 286 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541421B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-5d25c90e84924c199e87f72d7d77db23 |
| Source note | uspto-grants-2013_09 |