HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isothiocyanate → N-(2-Cyano-5-methylphenylcarbamothioyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isothiocyanate | HCID 68284 | — |
| Reactant | 2-Amino-4-methylbenzonitrile | HCID 2801276 | — |
| Product | N-(2-Cyano-5-methylphenylcarbamothioyl)benzamide | HCID 86625234 | — |
Reaction Steps
Prepared as in Example 1a from 2-amino-4-methylbenzonitrile and benzoyl isothiocyanate as a pale-yellow powder. 1H NMR (400 MHz, DMSO-d6) δ7.32 (d, J=8.0 Hz, 1H), 7.51-7.58 (m, 3H), 7.67 (t, J=7.8 Hz, 1H), 7.78 (d, J=8.0 Hz, 1H), 7.98-8.01 (m, 2H), 11.88 (s, 1H), 12.49 (s, 1H). MS 296 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541421B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-bba43de5a81047a1ba5c7172987ea55f |
| Source note | uspto-grants-2013_09 |