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10,11-Dihydro-11-oxodibenzo[b,f][1,4]thiazepin-3-carboxylic acid → HCID 13013940, compound

HRID 444161
Notes
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Reaction equation

HRID 444161 reaction equation
[O:1]=[C:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[S:6][C:5]2[CH:13]=[C:14]([C:17]([OH:19])=[O:18])[CH:15]=[CH:16][C:4]=2[NH:3]1.O=[C:21]1C2C=CC(C(O)=O)=CC=2SC2C=CC=CC=2N1>>[O:1]=[C:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[S:6][C:5]2[CH:13]=[C:14]([C:17]([O:19][CH3:21])=[O:18])[CH:15]=[CH:16][C:4]=2[NH:3]1
ParticipantsProcedureSources & evidenceReaction notes

Participants

3

Reactant 2

HCID 1301392310,11-Dihydro-11-oxodibenzo[b,f][1,4]thiazepin-3-carboxylic acidHCID 13013939HCID 13013939, compound

Product 1

HCID 13013940HCID 13013940, compound

Procedure

Repeat the process of Example 31, substituting 10,11-dihydro-11-oxodibenzo[b,f][1,4]thiazepin-7-carboxylic acid for the 10,11-dihydro-11-oxodibenzo[b,f][1,4]thiazepin-3-carboxylic acid of Step A, in order to obtain the title product.

Sources & evidence

ORD record
ord-efc2236fbf174213993b8eddacfe8544
Source dataset
uspto-grants-1981_04
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US04263207

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes