2-Chloro-4-fluorobenzaldehyde → HCID 58022610, compound

Reaction equation

[CH2:1]([C:3]1[CH:4]=[C:5]([SH:9])[CH:6]=[CH:7][CH:8]=1)[CH3:2].[Cl:10][C:11]1[CH:18]=[C:17](F)[CH:16]=[CH:15][C:12]=1[CH:13]=[O:14]>>[Cl:10][C:11]1[CH:18]=[C:17]([S:9][C:5]2[CH:6]=[CH:7][CH:8]=[C:3]([CH2:1][CH3:2])[CH:4]=2)[CH:16]=[CH:15][C:12]=1[CH:13]=[O:14]

Participants

Reactant 2

HCID 1450242-Chloro-4-fluorobenzaldehyde

HCID 155663113-Ethylbenzenethiol

Product 1

HCID 58022610HCID 58022610, compound

Procedure

3-Ethylbenzenethiol and 2-chloro-4-fluorobenzaldehyde were reacted according to the same experiment procedures as in Reference Example 1 of the pamphlet of WO 03029205 to obtain the target product as a colorless oil.

Sources & evidence

ORD record: ord-5c99921b9dc34856b11afe3f8d587ab5
Source dataset: uspto-grants-2013_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08476305B2

Reaction notes

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