Cyclohexanecarboxaldehyde → 1-Cyclohex-3-enyloxy-2,2,6,6-tetramethyl-piperidin-4-one

Reaction equation

[CH:1]1([O:7][N:8]2[C:13]([CH3:15])([CH3:14])[CH2:12][C:11](=[O:16])[CH2:10][C:9]2([CH3:18])[CH3:17])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C1(C=O)CCCCC1>>[CH:1]1([O:7][N:8]2[C:13]([CH3:14])([CH3:15])[CH2:12][C:11](=[O:16])[CH2:10][C:9]2([CH3:18])[CH3:17])[CH2:6][CH2:5][CH:4]=[CH:3][CH2:2]1

Participants

Reactant 2

HCID 16275Cyclohexanecarboxaldehyde

HCID 22019868N-cyclohexyloxy-4-oxo-2,2,6,6-tetramethylpiperidine

Product 1

HCID 583304141-Cyclohex-3-enyloxy-2,2,6,6-tetramethyl-piperidin-4-one

Procedure

1-Cyclohexyloxy-2,2,6,6-tetramethyl-piperidin-4-one, compound B, can be prepared in analogy using Cyclohexanecarboxaldehyde

Sources & evidence

ORD record: ord-9e06060f5bfd4eee96889e814b703b9c
Source dataset: uspto-grants-2013_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08481726B2

Reaction notes

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