Reaction equation
[CH:1]12[CH2:9][CH:5]3[CH2:6][CH:7]([CH2:8]1)[C:3]([NH:10][C:11]([NH2:13])=[S:12])([CH2:4]3)[CH2:2]2.Br[C:15]1([C:19](OCC)=[O:20])[CH2:18][CH2:17][CH2:16]1>>[CH:1]12[CH2:9][CH:5]3[CH2:6][CH:7]([CH2:8]1)[C:3]([NH:10][C:11]1[S:12][C:15]4([C:19](=[O:20])[N:13]=1)[CH2:18][CH2:17][CH2:16]4)([CH2:4]3)[CH2:2]2Participants
3
Procedure
Synthesis was performed from N-tricyclo[3.3.1.0˜3,7˜]non-3-ylthiourea and ethyl 1-bromocyclobutanecarboxylate according to Method D.
Workup
- customSynthesis
Sources & evidence
- ORD record
- ord-9caf7929b6af417c8f77091b32f10910
- Source dataset
- uspto-grants-2013_09
- Patent number
- US08541592B2
Linked notes
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