Diisopropylthiourea → HCID 22760621, compound

HRID 461158

Reaction equation

HRID 461158 reaction equation
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH:16]([NH:19][C:20]([NH:22][CH:23]([CH3:25])[CH3:24])=[S:21])([CH3:18])[CH3:17]>>[ClH:1].[CH:23]([N:22]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([CH3:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)([OH:4])[CH2:2][S:21][C:20]1=[N:19][CH:16]([CH3:18])[CH3:17])([CH3:25])[CH3:24]

Participants

3

Reactant 2

HCID 2758386DiisopropylthioureaHCID 136287832-Chloro-4'-methyl-3'-sulfamoylacetophenone

Product 1

HCID 22760621HCID 22760621, compound

Procedure

5 g of 2-chloro-4'-methyl-3'-sulfamoylacetophenone and 3.2 g of 1,3-diisopropyl thiourea were reacted as prescribed in Example 12 and worked up according to Example 67d). Colorless crystals, melting point: 152° C (decomposition).

Sources & evidence

ORD record
ord-7bac6b1dea9148f58fe92baf9ec13592
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Linked notes

Loading…